128960-28-1

Basic information

• Product Name: 2-<2-(p-bromobenzylidene)-1-methylhydrazino>-6-chloroquinoxaline 4-oxide
• CAS NO: 128960-28-1
• Molecular Weight: 391.654
• Mol File: 128960-28-1.mol
• Article Data: 2

Chemical Properties

• CAS DataBase Reference: 2-<2-(p-bromobenzylidene)-1-methylhydrazino>-6-chloroquinoxaline 4-oxide(CAS DataBase Reference)
• NIST Chemistry Reference: 2-<2-(p-bromobenzylidene)-1-methylhydrazino>-6-chloroquinoxaline 4-oxide(128960-28-1)
• EPA Substance Registry System: 2-<2-(p-bromobenzylidene)-1-methylhydrazino>-6-chloroquinoxaline 4-oxide(128960-28-1)

Safety Data

• Hazardous Substances Data: 128960-28-1(Hazardous Substances Data)

Upstream product

• 126983-41-3 6-chloro-2-[1-methyl-2-(2-thienylmethylene)hydrazino]quinoxaline-4-oxide 
• 1122-91-4 4-bromo-benzaldehyde 

Downstream Products

• 128980-89-2 3-(p-bromophenyl)-8-chloro-5-(2-hydroxyethoxy)-1-methyl-4-oxo-2,3,4,6-tetrahydro-1H-1,2-diazepino<3,4-b>quinoxaline 
• 128960-34-9 3-(p-bromophenyl)-8-chloro-5-ethoxy-1-methyl-4-oxo-2,3,4,6-tetrahydro-1H-1,2-diazepino<3,4-b>quinoxaline 
• 128960-31-6 3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride 
• 128960-32-7 3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline 

Relevant articles and documents

A Convenient Synthesis of 1,2-Diazepino-quinoxalines via a 1,3-Dipolar Cycloaddition Reaction and Their Tautomeric Structure in a Solution

The reaction of the quinoxaline 4-oxides 7a,b with 2-chloroacrylonitrile resulted in the 1,3-dipolar cycloaddition reaction and further alteration to give the 4-hydroxy-2,3-dihydro-1H-1,2-diazepinoquinoxalines 8a,b and 9a,b, respectively, which were converted into the 4-oxo-2,3,4,6-tetrahydro-1H-1,2-diazepinoquinoxalines 10a,b-12a,b, respectively.The 2,3-dihydro-4-hydroxy form of 9a,b and the 2,3,4,6-trtrahydro-4-oxo form of 10a,b-12a,b were assigned by means of the NOE and 13C-nmr spectral data.