13185-09-6Relevant articles and documents
Method for preparing 1-benzyl-3-hydroxy-1H-3-indazole sodium salt
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Paragraph 0007; 0026; 0027, (2017/08/31)
The invention relates to a method for preparing 1-benzyl-3-hydroxy-1H-3-indazole sodium salt. The method is characterized in that o-aminobenzoic acid, concentrated hydrochloric acid, a NaNO2 solution and solid Na2SO3 are taken as starting raw materials, a proper amount of a NaOH solution and a proper amount of benzyl chloride are added, and 1-benzyl-3-hydroxy-1H-3-indazole sodium salt is obtained through multi-step reaction filtering dehydration. The method is easily accessible in raw material, mild in reaction condition, low in cost and suitable for factory large-scale production.