13216-38-1

Basic information

• Product Name: 6-(4-chlorophenyl)-6,7-dihydro-5H-dibenzo[c,e]azepine
• Synonyms: 6-(4-chlorophenyl)-6,7-dihydro-5H-dibenzo[c,e]azepine
• CAS NO: 13216-38-1
• Molecular Weight: 305.807
• Mol File: 13216-38-1.mol
• Article Data: 2

Chemical Properties

• CAS DataBase Reference: 6-(4-chlorophenyl)-6,7-dihydro-5H-dibenzo[c,e]azepine(CAS DataBase Reference)
• NIST Chemistry Reference: 6-(4-chlorophenyl)-6,7-dihydro-5H-dibenzo[c,e]azepine(13216-38-1)
• EPA Substance Registry System: 6-(4-chlorophenyl)-6,7-dihydro-5H-dibenzo[c,e]azepine(13216-38-1)

Safety Data

• Hazardous Substances Data: 13216-38-1(Hazardous Substances Data)

Upstream product

• 1155858-61-9 C₂₀H₁₆ClI₂N 
• 3594-90-9 2,2'-bis(hydroxymethyl)biphenyl 
• 38274-14-5 2,2'-bis-(bromomethyl)-1,1'-biphenyl 
• 106-47-8 4-chloro-aniline 

Relevant articles and documents

Synthesis of 6,7-dihydro-5H-dibenzo[c,e]azepines and biaryls by palladium-catalyzed Ullmann reaction

A novel palladium-catalyzed Ullmann protocol is described for the synthesis of 6,7-dihydro-5H-dibenzo[c,e]azepines and biaryls. In the presence of Pd(OAc)2 and KOAc, intramolecular or intermolecular Ullmann coupling of aryl halides proceeds efficiently under ligand-free and aerobic conditions to afford the corresponding 6,7-dihydro-5H-dibenzo[c,e]azepines and biaryls in moderate to excellent yields.