142453-36-9Relevant articles and documents
Synthesis of 3-(6-Alkylaminopurin-9-yl)-2,3-dideoxy-D-threo-pentopyranoses and Their Reduction to 3-(6-Alkylaminopurin-9-yl)-2,3-dideoxy-D-threo-pentitols
Hjuler-Nielsen, Hans Peter,Pedersen, Hans,Hansen, Henning Bue,Pedersen, Erik B.,Nielsen, Claus
, p. 511 - 513 (2007/10/02)
3-(6-Alkylaminopurin-9-yl)-2,3-dideoxy-D-threo-pentopyranoses 3 were prepared by condensation of unprotected 2-deoxy-D-ribose (2) with N6-alkyladenines 1 in a phosphorus pentoxide reagent mixture.Reduction of the pentoses 3 gave the corresponding 3-(6-alkylaminopurin-9-yl)-2,3-dideoxy-D-threo-pentitols 4.The structures of 3 and 4 were determined by 13C nmr, 1H nmr and 2D 1H nmr (COSY).