155405-68-8

Basic information

• Product Name: 2-Chlor-N-(2-chlorbenzoyl)-N-(3-benzyl-2-pyridyl)benzamid
• Synonyms: 2-Chlor-N-(2-chlorbenzoyl)-N-(3-benzyl-2-pyridyl)benzamid
• CAS NO: 155405-68-8
• Molecular Weight: 461.347
• Mol File: 155405-68-8.mol
• Article Data: 1

Chemical Properties

• CAS DataBase Reference: 2-Chlor-N-(2-chlorbenzoyl)-N-(3-benzyl-2-pyridyl)benzamid(CAS DataBase Reference)
• NIST Chemistry Reference: 2-Chlor-N-(2-chlorbenzoyl)-N-(3-benzyl-2-pyridyl)benzamid(155405-68-8)
• EPA Substance Registry System: 2-Chlor-N-(2-chlorbenzoyl)-N-(3-benzyl-2-pyridyl)benzamid(155405-68-8)

Safety Data

• Hazardous Substances Data: 155405-68-8(Hazardous Substances Data)

Upstream product

• 3810-10-4 2-amino-3-benzoylpyridine 
• 609-65-4 o-chlorobenzoyl chloride 
• 130277-16-6 2-amino-3-benzylpyridine 

Downstream Products

• 155405-72-4 2-Chlor-N-(3-benzyl-2-pyridyl)benzamid 

Relevant articles and documents

Synthesis of 5H-pyrido[2,3-c]-2-benzazepines

The title compounds can be obtained by two different ways: Ring closure of 2-benzazepine enaminonitrile 1 and the C2-building blocks 2, 7 and 8 gives rise to the title compounds 6, 9 and 10. - The second way starts with Wolff-Kishner-reduction of the 2-amino-3-benzoylpyridines 16a,b to the 2-amino-3-benzylpyridines 18a,b. Benzoylation of 18a,b leads to the dibenzoylated compounds 20 and 21, respectively, which can be transformed to the monobenzoylated pyridines 22 resp. 23. Applying the Bischler-Napieralski-reaction on 22a,b and 23a,b leads to the 5H-pyrido[2,3-c]-2-benzazepines 24a,b and 25a,b. By means of 1H-, 13C- and 15N-NMR-data it is demonstrated that ethyl benzoylcyanacetimidate (12a) exists as benzoylketene-O,N-acetal 12a AE.