17696-89-8Relevant articles and documents
Preparation method of azodicarbonamide
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Paragraph 0029; 0050-0052; 0057-0059, (2021/12/07)
The preparation method comprises the following steps: Step S1, reacting hydrazine hydrochloride and dimethylbenzoyl chloride to form an intermediate. Step S2: The intermediate is subjected to an even nitridation reaction to give the azodicarboxamide. To the preparation method disclosed by the embodiment of the invention, the adopted raw material is high in safety, less in three wastes formed in production, and the obtained product can be obtained by effectively separating and drying, and pure product TMDA can be obtained without being purified again.
GEMINAL SYSTEMS. COMMUNICATION 29. REACTIONS OF N-CHLORO-N-METHOXY-N',N'-DIMETHYLUREA WITH N-NUCLEOPHILES
Rudchenko, V. F.,Shevchenko, V. I.,Kostyanovskii, R. G.
, p. 551 - 554 (2007/10/02)
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