86335-47-9Relevant articles and documents
Difunctionalized Trans-2,5-Disubstituted Pyrrolidine (Azethoxyl) Nitroxide Spin-Labels
Keana, John F. W.,Seyedrezai, Seyed E.,Gaughan, Glen
, p. 2644 - 2647 (1983)
The synthesis of two short-chain trans-2,5-difunctionalized azethoxyl nitroxide spin-labels, dinitrile 12 and dicarboxylic acid 14, is described.The trans stereochemistry of 12 and 14 was established by conversion of 12 to a diastereomeric mixture of N-hydroxy esters 13, which was analyzed by NMR spectroscopy.