96570-11-5Relevant articles and documents
Reaction of Ethyl β-Methoxycrotonate with some α,β-Unsaturated Carbonyl Compounds. Synthesis of 6-Aroyl-5-aryl-3-methoxycyclohex-2-enones
Shandala, Mowafak Y.,Ayoub, Mikdad T.,Kareem, Ahmad A.
, p. 1757 - 1759 (2007/10/02)
3-Aryl-1-phenyl-2-propen-1-ones Ia-h and 1-aryl-3-phenyl-2-propen-1-ones Ii-l reacted with ethyl β-methoxycrotonate (II) in the presence of sodium hydride in dry THF at 0 deg C for 10 hours to give the corresponding 6-aroyl-5-aryl-3-methoxy-2-cyclohexen-1-ones III.The structures of the products were confirmed by ir, pmr, (13)C nmr and uv spectroscopy.
