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1-Bromo-2-naphthol Bromonaphthol 2-Naphthalenol, 1-bromo-
Chemical Properties | off-white to beige or brown-purple cryst. powder |
Synthesis Reference(s) | Tetrahedron, 51, p. 4291, 1995 DOI: 10.1016/0040-4020(94)01119-K |
Purification Methods | Distil the naphthol at pKEst 10mm then recrystallise it from *C6H6/pet ether (b 30-60o) m 80-81o. The benzoyl derivative has m 98.5-99.5o (from MeOH). [Hazlet J Am Cherm Soc 62 2156 1940, Beilstein 6 H 650, 6 II 604, 6 III 2994.] |
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