10286-75-6

Basic information

• Product Name: N-(3,4-Dichlorophenyl)benzamide
• Synonyms: N-(3,4-Dichlorophenyl)benzamide;3',4'-DICHLOROBENZANILIDE
• CAS NO: 10286-75-6
• Molecular Formula: C₁₃H₉Cl₂NO
• Molecular Weight: 266.1227
• Mol File: 10286-75-6.mol
• Article Data: 9

Chemical Properties

• Melting Point: 145-146 °C
• Boiling Point: 304.7°Cat760mmHg
• Flash Point: 138.1°C
• Appearance: /
• Density: 1.384g/cm³
• Vapor Pressure: 0.00086mmHg at 25°C
• Refractive Index: 1.656
• PKA: 11.97±0.70(Predicted)
• CAS DataBase Reference: N-(3,4-Dichlorophenyl)benzamide(CAS DataBase Reference)
• NIST Chemistry Reference: N-(3,4-Dichlorophenyl)benzamide(10286-75-6)
• EPA Substance Registry System: N-(3,4-Dichlorophenyl)benzamide(10286-75-6)

Safety Data

• Hazardous Substances Data: 10286-75-6(Hazardous Substances Data)

Usage

InChI:InChI=1/C13H9Cl2NO/c14-11-7-6-10(8-12(11)15)16-13(17)9-4-2-1-3-5-9/h1-8H,(H,16,17)

Upstream product

• 6004-21-3 3'-chloro-benzanilide 
• 71144-20-2 (3,4-Dichloranilino)phenyl-acetonitril 
• 98-88-4 benzoyl chloride 
• 95-76-1 m,p-dichloroaniline 
• 99-54-7 3,4-dichloronitrobenzene 
• 65-85-0 benzoic acid 
• 20555-91-3 3,4-dichloroiodobenzene 
• 100-47-0 benzonitrile 
• 932-90-1 Benzaldoxime 
• 2399-66-8 1-benzoylpyrrolidin-2-one 
• 19226-36-9 3-phenyl-5H-1,4,2-dioxazol-5-one 
• 151169-75-4 3,4-dichlophenylboronic acid 

Downstream Products

• 10278-50-9 3',4'-dichlorothiobenzanilide 
• 344250-20-0 N-(3,4-dichlorophenyl)benzimidoyl chloride 
• 666175-14-0 1-[(3,4-dichlorophenylimino)phenylmethyl]-3-ethylthiourea 
• 95-76-1 m,p-dichloroaniline 
• 100-51-6 benzyl alcohol 

Relevant articles and documents

Copper-catalyzed regioselective synthesis of N-aryl amides from aldoximes and aryl halides

Ligand-assisted copper-catalyzed reaction of aldoximes with aryl halides is described for the regioselective synthesis of N-aryl amides. This protocol is simple and compatible with a wide range of functional groups attached to the aryl ring of the halides as well as aldoximes. Copyright

Visible-Light-Promoted Iron-Catalyzed N-Arylation of Dioxazolones with Arylboronic Acids

A visible-light-promoted and simple iron salt-catalyzed N-arylation was achieved efficiently under external photosensitizer-free conditions. Arylboronic acids and bench-stable dioxazolones were used for this cross-coupling reaction. This reaction features high reactivity, wide substrate scope, good functional group tolerance, simple operation procedure, and mild reaction conditions. Preliminary mechanistic investigations were conducted to support a radical pathway. This method may contribute to shift the paradigm of iron-catalyzed C-N bond construction and nitrene transfer chemistry.

Copper-Catalyzed Regioselective Synthesis of N-Aryl Amides from Aldoximes and Aryl Halides

Ligand-assisted copper-catalyzed reaction of aldoximes with aryl halides is described for the regioselective synthesis of N-aryl amides. This protocol is simple and compatible with a wide range of functional groups attached to the aryl ring of the halides as well as aldoximes.