1068439-06-4Relevant articles and documents
Novel and efficient methods for the synthesis of symmetrical trisulfides
Kertmen, Ahmet,Lach, Slawomir,Rachon, Janusz,Witt, Dariusz
, p. 1459 - 1462 (2009)
We have developed convenient methods for the synthesis of symmetrical trisulfides under mild conditions in very good yields. The described methods are based on the straightforward preparation of (5,5-dimethyl-2-thioxo-1,3,2- dioxaphosphorin-2-yl)disulfany
DDQ-mediated synthesis of functionalized unsymmetrical disulfanes
Musiejuk, Mateusz,Klucznik, Tomasz,Rachon, Janusz,Witt, Dariusz
, p. 31347 - 31351 (2015/04/22)
We developed a simple and efficient method for the synthesis of functionalized unsymmetrical disulfanes under mild conditions in good yields. The designed method is based on the reaction of bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)disulfane with thiols in the presence of 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ). The developed method allows the preparation of unsymmetrical disulfanes bearing additional hydroxy, carboxy, or amino functionalities.