1122-55-0Relevant articles and documents
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Brady,W.T.,Patel,A.D.
, p. 565 (1972)
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A novel method for the synthesis of dichloroalkenes
Nenajdenko,Shastin,Muzalevskii,Balenkova
, p. 2647 - 2649 (2007/10/03)
A novel convenient method for the synthesis of dichloroalkenes was developed. The method involves catalytic olefination of hydrazones of aliphatic carbonyl compounds with bromo(trichloro)methane.
ACETONITRILE: AN EXCELLENT SOLVENT FOR THE 1,1-DICHLOROMETHYLENATION OF CERTAIN KETONES
Burton, George,Elder, John S.,Fell, Stephen C. M.,Stachulski, Andrew V.
, p. 3003 - 3006 (2007/10/02)
Cyclohexanones react rapidly at or below room temperature with Ph3P and XCCl3 (X=Br or Cl) in acetonitrile to give 1,1-dichloromethylenecompounds in high yield; some α-methoxyimino β-(1,1-dichloro)methylene esters have been similarly prepared.