113283-89-9Relevant articles and documents
Microwave-assisted carbamoylation of amines
Azzena, Ugo,Dettori, Giovanna,Pisano, Luisa,Pittalis, Mario
, p. 3623 - 3634 (2008/03/13)
The influence of microwave irradiation on the reaction of various amines with benzyl chloroformate and di-tert-butyl dicarbonate was investigated. Microwave irradiation was successfully applied to the carbamoylation of several nonfunctionalized and functionalized amines, including amino acids and nucleobases, leading to satisfactory to high product conversion within very short reaction times. Copyright Taylor & Francis Group, LLC.
Selective Protection of Mixed Primary-Secondary Amines. Simple Preparation of N1,N8-Bis(t-butoxycarbonyl)spermidine
Lurdes, M.,Almeida, S.,Grehn, Leif,Ragnarsson, Ulf
, p. 1250 - 1251 (2007/10/02)
A new, simple, and efficient preparative procedure of a potentially wide scope for the selective protection of mixed primary-secondary amines, based on acylation followed by exhaustive t-butoxycarbonylation is presented.