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117-62-4

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117-62-4 Usage

Chemical Properties

BEIGE POWDER

Check Digit Verification of cas no

The CAS Registry Mumber 117-62-4 includes 6 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 3 digits, 1,1 and 7 respectively; the second part has 2 digits, 6 and 2 respectively.
Calculate Digit Verification of CAS Registry Number 117-62:
(5*1)+(4*1)+(3*7)+(2*6)+(1*2)=44
44 % 10 = 4
So 117-62-4 is a valid CAS Registry Number.
InChI:InChI=1/C10H9NO6S2/c11-8-5-4-6-7(10(8)19(15,16)17)2-1-3-9(6)18(12,13)14/h1-5H,11H2,(H,12,13,14)(H,15,16,17)/p-2

117-62-4Synthetic route

6-aminonaphthalene-1-sulfonic acid
81-05-0

6-aminonaphthalene-1-sulfonic acid

A

6-amino-naphthalene-1,3-disulfonic acid
118-33-2

6-amino-naphthalene-1,3-disulfonic acid

B

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

Conditions
ConditionsYield
With sulfuric acid at 20℃;
With sulfuric acid
2-aminonaphthalenesulfonic acid
81-16-3

2-aminonaphthalenesulfonic acid

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

Conditions
ConditionsYield
With sulfuric acid at 30 - 40℃;
With sulfuric acid
sulfuric acid
7664-93-9

sulfuric acid

2-aminonaphthalenesulfonic acid
81-16-3

2-aminonaphthalenesulfonic acid

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

sulfuric acid
7664-93-9

sulfuric acid

6-aminonaphthalene-1-sulfonic acid
81-05-0

6-aminonaphthalene-1-sulfonic acid

A

6-amino-naphthalene-1,3-disulfonic acid
118-33-2

6-amino-naphthalene-1,3-disulfonic acid

B

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

4-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-5-hydroxy-naphthalene-2,7-disulfonic acid
7538-88-7

4-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-5-hydroxy-naphthalene-2,7-disulfonic acid

C23H14Cl2N6O13S4
57583-84-3

C23H14Cl2N6O13S4

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite at 8 - 10℃; for 1h; pH=6 - 6.5;65%
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

1,2-Naphthochinon-2-diazid-5-sulfonsaeure
94386-30-8

1,2-Naphthochinon-2-diazid-5-sulfonsaeure

Conditions
ConditionsYield
Behandlung mit Soda.Diazotization;
Behandlung mit Soda in Gegenwart von Oxydationsmitteln.Diazotization;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

1,6-dihydroxynaphthalene
575-44-0

1,6-dihydroxynaphthalene

Conditions
ConditionsYield
at 240℃; bei der Kalischmelze unter Druck;
Multi-step reaction with 2 steps
1: durch Kalischmelze
2: 240 °C / bei der Kalischmelze unter Druck
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

7-aminonaphthalene-2-sulfonic acid
494-44-0

7-aminonaphthalene-2-sulfonic acid

Conditions
ConditionsYield
With sulfuric acid at 130℃;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

2-amino-5-hydroxy-naphthalene-1-sulfonic acid
871887-69-3

2-amino-5-hydroxy-naphthalene-1-sulfonic acid

Conditions
ConditionsYield
With potassium hydroxide
With potassium hydroxide at 210 - 230℃;
durch Kalischmelze;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

6-aminonaphthalene-1-sulfonic acid
81-05-0

6-aminonaphthalene-1-sulfonic acid

Conditions
ConditionsYield
With sulfuric acid
With sulfuric acid at 100 - 107℃;
With sulfuric acid
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

2-Aminonaphthalene-1,5,7-trisulfonic acid
55524-84-0

2-Aminonaphthalene-1,5,7-trisulfonic acid

Conditions
ConditionsYield
With sulfuric acid
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

2,5-dihydroxy-naphthalene-1-sulfonic acid
858464-85-4

2,5-dihydroxy-naphthalene-1-sulfonic acid

Conditions
ConditionsYield
With potassium hydroxide; water at 240℃;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

2-chloro-naphthalene-1,5-disulfonic acid
102878-17-1

2-chloro-naphthalene-1,5-disulfonic acid

Conditions
ConditionsYield
durch Ersatz von NH2 durch Cl nach dem SANDMEYERschen Verfahren;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

1,5-disulfo-naphthalene-2-diazonium-betaine
744985-01-1

1,5-disulfo-naphthalene-2-diazonium-betaine

Conditions
ConditionsYield
Diazotization.angewandt als saures Natriumsalz;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

Bronner acid
93-00-5

Bronner acid

Conditions
ConditionsYield
With sulfuric acid at 130℃;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

1-naphthol-7-(2',4'-dichloro-s-triazin-6'-ylamino)-3-sulphonic acid
151618-94-9

1-naphthol-7-(2',4'-dichloro-s-triazin-6'-ylamino)-3-sulphonic acid

1-naphthol-2-(1',5'-disulphonaphthyl-2-azo)-7-(2'',4''-dichloro-s-triazin-6''-ylamino)-3-sulphonic acid
163404-56-6

1-naphthol-2-(1',5'-disulphonaphthyl-2-azo)-7-(2'',4''-dichloro-s-triazin-6''-ylamino)-3-sulphonic acid

Conditions
ConditionsYield
With sodium carbonate 2.) 0-5 deg C, 3 h; Multistep reaction;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

potassium hydroxide

potassium hydroxide

2-amino-5-hydroxy-naphthalene-1-sulfonic acid
871887-69-3

2-amino-5-hydroxy-naphthalene-1-sulfonic acid

Conditions
ConditionsYield
at 210 - 230℃;
sulfuric acid
7664-93-9

sulfuric acid

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

6-aminonaphthalene-1-sulfonic acid
81-05-0

6-aminonaphthalene-1-sulfonic acid

sulfuric acid
7664-93-9

sulfuric acid

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

A

6-aminonaphthalene-1-sulfonic acid
81-05-0

6-aminonaphthalene-1-sulfonic acid

B

naphthalen-2-ylamine
91-59-8

naphthalen-2-ylamine

sulfuric acid
7664-93-9

sulfuric acid

2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

A

7-aminonaphthalene-2-sulfonic acid
494-44-0

7-aminonaphthalene-2-sulfonic acid

B

6-aminonaphthalene-1-sulfonic acid
81-05-0

6-aminonaphthalene-1-sulfonic acid

C

Bronner acid
93-00-5

Bronner acid

Conditions
ConditionsYield
at 130℃;
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

6-aminonaphthalen-1-ol
23894-12-4

6-aminonaphthalen-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: durch Kalischmelze
2: diluted acid / 145 - 150 °C / unter Druck
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

N-(5-hydroxynaphthalen-2-yl)acetamide
86700-06-3

N-(5-hydroxynaphthalen-2-yl)acetamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: durch Kalischmelze
2: diluted acid / 145 - 150 °C / unter Druck
3: sodium acetate
4: natrium carbonate
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

N-(5-hydroxy-[2]naphthyl)-benzamide

N-(5-hydroxy-[2]naphthyl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: durch Kalischmelze
2: diluted acid / 145 - 150 °C / unter Druck
3: NaOH-solution
4: alcoholic KOH-solution
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

6-benzoylamino-1-benzoyloxy-naphthalene

6-benzoylamino-1-benzoyloxy-naphthalene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: durch Kalischmelze
2: diluted acid / 145 - 150 °C / unter Druck
3: NaOH-solution
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

2-acetylamino-5-hydroxy-naphthalene-1-sulfonic acid

2-acetylamino-5-hydroxy-naphthalene-1-sulfonic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: durch Kalischmelze
2: sodium acetate / 30 - 40 °C
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

5,5'-dihydroxy-2,2'-ureylene-bis-naphthalene-1-sulfonic acid
861333-75-7

5,5'-dihydroxy-2,2'-ureylene-bis-naphthalene-1-sulfonic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: durch Kalischmelze
2: natrium carbonate
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

1-acetoxy-6-acetylamino-naphthalene

1-acetoxy-6-acetylamino-naphthalene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: durch Kalischmelze
2: diluted acid / 145 - 150 °C / unter Druck
3: sodium acetate
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

6-amino-1-hydroxy-naphthalene-2-sulfonic acid

6-amino-1-hydroxy-naphthalene-2-sulfonic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: durch Kalischmelze
2: concentrated sulfuric acid / 40 °C
3: sulfuric acid
View Scheme
Multi-step reaction with 3 steps
1: durch Kalischmelze
2: concentrated sulfuric acid / 20 °C
3: sulfuric acid
View Scheme
2-amino-1,5-naphthalenedisulfonic acid
117-62-4

2-amino-1,5-naphthalenedisulfonic acid

7-amino-4-hydroxy-naphthalene-1,3-disulfonic acid
861353-37-9

7-amino-4-hydroxy-naphthalene-1,3-disulfonic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: durch Kalischmelze
2: concentrated sulfuric acid / 40 °C
View Scheme

117-62-4Relevant articles and documents

High temperature process for preparing fiber reactive dyes

-

, (2008/06/13)

A process for preparing monoazo dyes by coupling a aromatic diazonium salt with an amino-4-hydroxy-naphthalene sulfonic acid derivative at a temperature of 40°-85° C. The process of the invention provides a isomerically purer dye.

Fiber reactive monoazo compounds having two vinylsulfone type fiber reactive groups in the molecule

-

, (2008/06/13)

A monoazo compound of the following formula in a free acid form, STR1 wherein A1 and A2 are phenylene or naphthylene, Z1 and Z2 are --SO2 CH=CH2 or --SO2 CH2 CH2 Y in which Y is a splittable group, R1 and R2 are hydrogen or alkyl, and D is sulfophenyl or sulfonaphthyl, provided that --A1 --Z1 and --A2 --Z2 are different from each other when D is sulfophenyl and both R1 and R2 are hydrogen, which is useful for dyeing or printing fiber materials to give dyed products of high fastness properties with extremely high color depth.

Reactive yellow dye having both monochlorotriazinyl and vinylsulfone type reactive groups

-

, (2008/06/13)

The compounds represented, in the form of free acid, by the following general formula (I): STR1 (wherein A is STR2 (wherein R3 and R4 are each hydrogen or a methyl, ethyl, methoxy, ethoxy, acetylamino, propionylamino, benzoylamino or ureido group, and R5 and R6 are each hydrogen or a methyl or methoxy group), R1 and R2 are each hydrogen or a methyl, ethyl or sulfomethyl group, X1 and X2 are each hydrogen, chlorine or a methyl, methoxy, carboxyl or sulfonic acid group, m is a number of 0, 1 or 2, and n is a number of 1 or 2, provided that the sum of m and n is 1, 2 or 3). These compounds are capable of dyeing cellulose fibers in yellow with excellent color fastness to hypochlorite, light, perspiration and sunlight and high acid stability.

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