1192763-61-3Relevant articles and documents
Electrocyclization-mediated approach to 2-methyltriclisine, an unnatural analog of the azafluoranthene alkaloid triclisine
Silveira, Claudio C.,Larghi, Enrique L.,Mendes, Samuel R.,Bracca, Andrea B. J.,Rinaldi, Francieli,Kaufman, Teodoro S.
, p. 4637 - 4645 (2009)
The synthesis of 2-methyltriclisine, an unnatural analog of the azafluoranthene alkaloid, triclisine, is reported. The synthesis was achieved in 10 steps and 21% overall yield from 2-bromo-3,4-dimethoxybenzaldehyde, through the intermediacy of 3,4-dimetho