1207379-31-4Relevant articles and documents
Hexamethylenetetramine-based ionic liquid/MIL-101(Cr) metal-organic framework composite: a novel and versatile tool for the preparation of pyrido[2,3-d:5,6-d′]dipyrimidines
Mirhosseini-Eshkevari, Boshra,Ghasemzadeh, Mohammad Ali,Esnaashari, Manzarbanoo,Ganjali, Saeed Taghvaei
, p. 364 - 373 (2021/02/09)
In the current paper, a hexamethylenetetramine-based ionic liquid immobilized on the MIL-101(Cr) metal-organic framework was successfully synthesized as a novel, efficient, and recoverable catalyst for the synthesis of pyrido[2,3-d:5,6-d′]dipyrimidine derivativesviathe reaction of barbituric acid derivatives, 6-aminouracil/6-amino-1,3-dimethyl uracil, and aromatic aldehydes under solvent-free conditions. Characterization of the catalyst was carried out using various methods such as field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD), thermogravimetric analysis (TGA), Fourier transform infrared spectrophotometry (FT-IR), and Brunauer-Emmett-Teller (BET). Efficient transformation, short reaction times, excellent yields, easy product isolation, mild conditions, and the potential high recyclability of the organocatalyst are the main features of this protocol.
Three-component green reaction of arylaldehydes, 6-Amino-1,3-dimethyluracil and active methylene compounds catalyzed by Zr(HSO4)4 Under solvent-free conditions
Abdolmohammadi, Shahrzad,Balalaie, Saeed,Barari, Mohammad,Rominger, Frank
, p. 150 - 159 (2013/07/28)
A convenient one-pot, three-component reaction of aromatic aldehydes, 6-amino-1,3-dimethyluracil and active methylene compounds in the presence of Zr(HSO4)4 as a heterogeneous catalyst, under solvent-free conditions brings a very sim