1228539-19-2Relevant articles and documents
Microwave-assisted synthesis of nitro-substituted tetrahydropyrido azepines
Schultz, Thomas,Turner, Sean C.,Braje, Wilfried M.
experimental part, p. 1339 - 1343 (2010/07/06)
The microwave-assisted condensation of azepan-4-ones with 3,5-dinitro-1-methylpyridin-2-one in the presence of ammonia was found to be a highly efficient method for the synthesis of nitro-substituted tetrahydropyridoazepines. Variation of the substituent at the amino group enables the regioselective synthesis of tetrahydropyrido[3,2-c]azepines and tetrahydropyrido[2,3-d]azepines. Georg Thieme Verlag Stuttgart · New York.
