1258930-42-5Relevant articles and documents
A facile and practical solvent-free one-pot synthesis of (Z)-4-methylene-3-selenaquinoline derivatives from o-ethynylanilines and isoselenocyanates
Sashida, Haruki,Pan, Chao,Kaname, Mamoru,Minoura, Mao
experimental part, p. 3091 - 3096 (2010/10/21)
Heating of o-ethynylanilines with isoselenocyanates directly resulted in the 6-exo-dig mode ring-closure reaction of the adducts to give the (Z)-2-imino-4-methylene-3-selenaquinolines in moderate to good yields. Based on this convenient, solvent-free, catalyst-free method, several 3-selenaquinoline derivatives (3,1-benzoselenazines) were easily obtained in one pot. Successful application of the microwave-assisted synthesis of these compounds was also investigated. Georg Thieme Verlag Stuttgart - New York.