1310466-22-8Relevant articles and documents
Preparation method of 4-(2-methylallyl)-1,2-benzenediol
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Paragraph 0023; 0024, (2017/08/29)
The invention discloses a preparation method of 4-(2-methylallyl)-1,2-benzenediol. The preparation method comprises the following steps: taking gamma-aluminum oxide as a catalyst for catalyzing 2-(2-methyl allyloxy) phenol so as to continuously carry out Claisen rearrangement and Cope rearrangement reaction in an organic solvent, and generating the 4-(2-methylallyl)-1,2-benzenediol. The preparation method of the 4-(2-methylallyl)-1,2-benzenediol, disclosed by the invention, has the advantages of high yield, high purity, simpleness in operation, convenience for recycling and reusing the catalyst, low cost, environment protecting and the like.