133710-22-2Relevant articles and documents
CHEMICO-ENZYMATIC SYNTHESES OF RACEMIC AND CHIRAL ISOMERS OF 7-METHYL-1,6-DIOXASPIRODECANE
Ramaswamy, Sowmianarayanan,Oehlschlager, Allan C.
, p. 1157 - 1162 (2007/10/02)
Porcine pancreatic lipase (PPL) mediated resolution of 6-heptene-2-ol afforded the enantiomers in high optical purities.Alkylation products of the dianion of the 2-4'-hydroxypentyl-1,3-dithiane prepared from the enantiomers, followed by alkylative hydrolysis, afforded 97percent optically pure E-7-methyl-1,6-dioxaspirodecane.