13400-67-4

Basic information

• Product Name: 3,7-dioxo-5α-cholestane
• Synonyms: 3,7-dioxo-5α-cholestane
• CAS NO: 13400-67-4
• Molecular Weight: 400.645
• Mol File: 13400-67-4.mol
• Article Data: 4

Chemical Properties

• CAS DataBase Reference: 3,7-dioxo-5α-cholestane(CAS DataBase Reference)
• NIST Chemistry Reference: 3,7-dioxo-5α-cholestane(13400-67-4)
• EPA Substance Registry System: 3,7-dioxo-5α-cholestane(13400-67-4)

Safety Data

• Hazardous Substances Data: 13400-67-4(Hazardous Substances Data)

Upstream product

• 809-51-8 7-ketocholesteryl acetate 
• 40823-16-3 acetic acid-(7β-hydroxy-5α-cholestanyl-(3β)-ester) 
• 566-28-9 7-Oxocholesterol 
• 57-88-5 cholesterol 
• 6038-71-7 3β-acetoxy-5α-cholestan-7-one 
• 7591-17-5 3β-hydroxy-5α-cholestan-7-one 
• 64-19-7 acetic acid 
• 566-25-6 5α-cholestane-3β,7β-diol 
• 22420-06-0 Δ⁶-3β-cholestenol 
• 145800-90-4 6β-Iodo-5-iodomethyl-4-nor-5β-cholestane-3,7-dione 
• 566-88-1 dihydrocholesterone 

Downstream Products

• 1621062-74-5 3α,7α-di(phenylamino)-5α-cholestane 
• 1621062-76-7 3β,7α-di(phenylamino)-5α-cholestane 
• 1621062-73-4 3α-phenylamino-5α-cholestan-7-one 
• 1621062-75-6 3β-phenylamino-5α-cholestan-7-one 
• 1621062-91-6 3α,7α-di[(4-nitrophenyl)amino]-5α-cholestane 
• 1621062-92-7 3β,7α-di[(4-nitrophenyl)amino]-5α-cholestane 
• 1621062-86-9 3β,7α-di[(3-bromophenyl)amino]-5α-cholestane 
• 1621062-85-8 3α,7α-di[(3-bromophenyl)amino]-5α-cholestane 
• 1621062-83-6 3α,7α-di[(4-bromophenyl)amino]-5α-cholestane 
• 1621062-84-7 3β,7α-di[(4-bromophenyl)amino]-5α-cholestane 
• 1621062-81-4 3α,7α-di[(2-aminophenyl)amino]-5α-cholestane 
• 1621062-79-0 3α,7α-di[(4-methoxyphenyl)amino]-5α-cholestane 
• 1621062-80-3 3β,7α-[di(4-methoxyphenyl)amino]-5α-cholestane 
• 1621062-78-9 3β,7α-di[(4-methylphenyl)amino]-5α-cholestane 

Relevant articles and documents

The synthesis of facial amphiphile 3α,7α-diaminocholestane

The facial amphiphile 3α,7α-diaminocholestane 3 was synthesized from 3β-acetoxy-7-ketocholestane 1 through a stepwise reductive amination. The reductive amination of 1 with NH4OAc in the presence of NaBH3CN, and protection with Boc2O yielded 7α-(tert-butyloxycarbonyl)-aminocholestane 4 in 86% yield. The reductive amination of 6, which was obtained from 4 after hydrolysis and subsequent oxidation, with NH4OTf in the presence of NaBH(OEh)3 provided 3 in 75% yield after protection with Boc2O.

Photoinduced Molecular Transformations. Part 136. Reactions of Alkoxyl Radicals generated from Hypoiodites of 3β-Hydroxy-7-oxo-Δ5-Steroids. Synthesis of Some Functionalized Oxasteroids

The synthesis of several unsaturated 3-oxasteroids and 4a-homo-4-oxasteroids of cholestane series functionalized at their B-ring is described; 3β-hydroxycholest-5-en-7-one and its 4,4-dimethyl derivative were transformed into 3-oxacholest-5-en-7-one and i