1352877-24-7Relevant articles and documents
Piecing together the puzzle: Understanding a mild, metal free reduction method for the large scale synthesis of hydrazines
Browne, Duncan L.,Baxendale, Ian R.,Ley, Steven V.
supporting information; experimental part, p. 10296 - 10303 (2012/01/04)
A key intermediate for the synthesis of hydrazines via a mild, metal free reduction of diazonium salts has been isolated and characterized by X-ray analysis. The presence of this intermediate is general, as demonstrated by the preparation of a number of analogues. A discussion of the mechanism and potential benefits of such a process are also described.