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An efficient stereospecific method for the synthesis of 8-aza-3-deazaguanine nucleosides from glycosyl azides
?timac, Anton,Leban, Ivan,Kobe, Jo?e
, p. 1069 - 1073 (2007/10/03)
8-aza-3-deazaguanine nucleosides 8 were prepared from glycosyl azides 1 via a stereospecific Dimroth reaction with dimethyl 3-oxoglutarate, followed by selective manipulation of the 1,2,3-triazole C-4 and 5 substituents. Of the two methods evaluated for t