13688-56-7Relevant articles and documents
N,N'-Bis-urea: A Useful Silylating Agent for Alcohols and Carboxylic Acids
Verboom, W.,Visser, G. W.,Reinhoudt, D. N.
, p. 807 - 809 (1981)
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PROCESS FOR SILYLATING MONOCARBOXYLIC ACIDS
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Page/Page column 4, (2010/06/22)
A process for preparing silylated monocarboxylic acids by reacting C2-C10-monocarboxylic acids with halosilanes of the general formula (I) SiHal4-xRx??(I) in which Hal is a halogen atom selected from the group of fluorine, chlorine, bromine and iodine, R is independently hydrogen, Cl-C10-alkyl or aryl and x is an integer of 0 to 3 to form hydrogen halide in the presence of an auxiliary base, wherein the auxiliary base and the hydrogen halide form a salt which forms two immiscible phases with the product of value or the solution of the product of value in a suitable solvent and is removed.
Reagents and Synthetic Methods; 14. A Facile Synthesis of Carboxylic Acid Bromides and Esters under Neutral Conditions via Reaction of the Trimethylsilyl Esters with Triphenylphosphine Dibromide
Aizpurua, Jesus Mari,Palomo, Claudio
, p. 684 - 686 (2007/10/02)
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