147670-94-8Relevant articles and documents
FIVE-MEMBERED 2,3-DIOXOHETEROCYCLES. XXIII. SYNTHESIS OF 1-ARYL-3-AROYL-4,5-DIHYDRO-4,5-PYRAZOLEDIONES AND THEIR REACTION WITH WATER AND ALCOHOLS
Pimenova, E. V.,Andreichikov, Yu. S.
, p. 302 - 315 (2007/10/02)
4-Aroyl-3-arylhydrazono-2,4-dioxobutyric acids were obtained by the azo coupling of aroylpyruvic acids with arenediazonium salts. Under the influence of thionyl chloride (benzene, 78 deg C, 1.5-4h) they undergo cyclization to 1-aryl-3-aroyl-4,5-dihydro-4,