16717-84-3Relevant articles and documents
New halogenation reagent system for one-pot conversion of alcohols into iodides and azides
Kamal, Ahmed,Ramesh,Laxman
, p. 827 - 833 (2001)
In Situ generation of hydrogen iodide from methanesulphonic acid/sodium iodide in different solvents was found to be an attractive reagent system for the chemoselective conversion of various alcohols to their corresponding iodides. Moreover, treatment of benzylic and allylic alcohols with this reagent system, followed by substitution with azide ion, produced the corresponding azides in one pot in good yields.
Direct catalytic azidation of allylic alcohols
Rueping, Magnus,Vila, Carlos,Uria, Uxue
supporting information; experimental part, p. 768 - 771 (2012/03/26)
A direct catalytic azidation of primary, secondary, and tertiary allylic alcohols has been developed. This new azidation reaction affords the corresponding allylic azides in high to excellent yields and regioselectivities. The reaction provides straightforward access to allylic azides that are valuable intermediates in organic synthesis, including the preparation of primary amines or 1,2,3-triazole derivatives.
A simple one-pot method for the preparation of allyl azides from allyl alcohols using triphosgene: Synthesis of N1-cinnamyl azetidin-2-ones
Jayanthi,Gumaste,Deshmukh
, p. 979 - 982 (2007/10/03)
A simple and efficient one-pot method for the preparation of allyl azides from allyl alcohols using triphosgene and sodium azide is described. An application of cinnamyl azide for the synthesis of various N1 -cinnamyl azetidin-2-ones is also described.
