183448-68-2Relevant articles and documents
Novel synthesis of stable furan and thiophene o-amino thioaldehydes by reaction of o-azido aldehydes with hexamethyldisilathiane
Capperucci, Antonella,Degl'Innocenti, Alessandro,Funicello, Maria,Scafato, Patrizia,Spagnolo, Piero
, p. 1185 - 1187 (2007/10/03)
A new synthesis of monomeric o-amino thioaldehydes of thiophene, benzo[b]thiophene, furan and benzo[b]furan by reacting the corresponding o-azido aldehydes with hexamethyldisilathiane in neat acetonitrile and/or in methanol in the presence of hydrochloric acid at room temperature is reported.