191528-63-9Relevant articles and documents
The synthesis of a novel benzodiazocine via an intramolecular Staudinger/aza-Wittig cyclization
O'Neil, Ian A.,Murray, Clare L.,Potter, Andrew J.,Kalindjian, S. Barret
, p. 3609 - 3610 (2007/10/03)
The novel pyrrolobenzodiazocine (1) has been prepared by an intramolecular Staudinger/aza Wittig protocol from the precursor azido aldehyde (2) in a remarkable 93% yield. Aldehyde (2) was prepared by coupling protected homoprolinol with 2-azidobenzoic aci