208194-62-1Relevant articles and documents
A facile one-pot synthesis of α-bromo-α,β-unsaturated esters from alcohols
Karama, Usama,Al-Othman, Zeid,Al-Majid, Abdullah,Almansour, Abdulrahman
experimental part, p. 3276 - 3280 (2010/09/05)
Treatment of N-bromosuccinimide (NBS) with (carboethoxymethylene) triphenylphosphorane (1) in CH2Cl2 followed by the addition of an alcohol in the presence of manganese dioxide under ultrasonic irradiation constitutes a stereoselective one-pot procedure for the preparation of Z-configured α-bromo-α,β-unsaturated esters in good to excellent yield.