274905-50-9Relevant articles and documents
A new, efficient entry to nucleoside 2',3'-O,O-cyclophosphorothioates
Jankowska, Jadwiga,Wenska, Malgorzata,Popenda, Mariusz,Stawiński, Jacek,Kraszewski, Adam
, p. 2227 - 2229 (2007/10/03)
The reaction of 5'-protected ribonucleosides with diphenyl H-phosphonate in pyridine furnished rapid formation of the corresponding 2',3'-cyclic H- phosphonates 3, which upon sulfurisation and the subsequent removal of the 5'-protecting group, afforded nucleoside 2',3'-O,O-cyclophosphorothioates 5 in high yields. (C) 2000 Elsevier Science Ltd.