28567-36-4Relevant articles and documents
Highly efficient protection of alcohols as trityl ethers under solvent-free conditions, and recovery catalyzed by reusable nanoporous MCM-41-SO3H
Gholamzadeh, Zeynab,Naimi-Jamal, Mohammad Reza,Maleki, Ali
, p. 994 - 1001 (2015/01/09)
An efficient method was developed for the protection of alcohols as trityl ethers using triphenylmethanol in the presence of nanoporous MCM-41-SO3H as a heterogeneous catalyst under solvent-free ball-milling at room temperature. Low catalyst loading, high efficiency, reusability are among the advantages of this new solvent-free and environmentally friendly method. The deprotection of the produced trityl ethers was also efficiently achieved using the same catalyst in wet acetonitrile.
FeCl3-catalyzed tritylation of alcohols in ionic liquids
Sreedhar,Radhika,Neelima,Chowdary,Rao, M. V. Basaveswara
experimental part, p. 3785 - 3795 (2009/12/08)
A simple and efficient protection of alcohols as trityl ethers is described using trityl chloride in the presence of 5mol% FeCl3 as catalyst in ionic liquids at room temperature in shorter reaction times. This mild and efficient method gives access to the
