32654-60-7

Basic information

• Product Name: 3,5-Dinitro-4-aminophenol
• Synonyms: 3,5-Dinitro-4-aminophenol;4-Amino-3,5-dinitrophenol
• CAS NO: 32654-60-7
• Molecular Formula: C₆H₅N₃O₅
• Molecular Weight: 199.121
• Mol File: 32654-60-7.mol
• Article Data: 1

Chemical Properties

• Boiling Point: 429.4°Cat760mmHg
• Flash Point: 213.5°C
• Appearance: /
• Density: 1.749g/cm³
• Vapor Pressure: 5.62E-08mmHg at 25°C
• Refractive Index: 1.73
• CAS DataBase Reference: 3,5-Dinitro-4-aminophenol(CAS DataBase Reference)
• NIST Chemistry Reference: 3,5-Dinitro-4-aminophenol(32654-60-7)
• EPA Substance Registry System: 3,5-Dinitro-4-aminophenol(32654-60-7)

Safety Data

• Hazardous Substances Data: 32654-60-7(Hazardous Substances Data)

Usage

InChI:InChI=1/C6H5N3O5/c7-6-4(8(11)12)1-3(10)2-5(6)9(13)14/h1-2,10H,7H2

Upstream product

• 731772-53-5 5-acetoxy-2-acetylamino-1,3-dinitrobenzene 
• 856207-50-6 methanesulfonic acid-(4-ethoxy-2,6-dinitro-anilide) 
• 876476-95-8 ethanesulfonic acid-(4-ethoxy-2,6-dinitro-anilide) 
• 872265-28-6 toluene-4-sulfonic acid-(4-hydroxy-2,6-dinitro-anilide) 
• 861560-22-7 2-nitro-toluene-4-sulfonic acid-(4-ethoxy-2,6-dinitro-anilide) 
• 7647-01-0 hydrogenchloride 
• 7664-93-9 sulfuric acid 
• 7403-13-6 acetic acid-(4-hydroxy-2.6-dinitro-anilide) 
• 450365-10-3 1-acetoxy-4-(toluene-4-sulfonylamino)-benzene 
• 108-24-7 acetic anhydride 
• 80824-77-7 4'-(benzyloxy)benzanilide 
• 15457-50-8 p-benzoylaminophenol 
• 10406-66-3 methanesulfonic acid p-phenetidide 
• 74973-18-5 acetic acid 4-benzoylaminophenyl ester 

Downstream Products

• 586-11-8 3,5-dinitrophenol 
• 408329-12-4 acetic acid-(4-hydroxy-2,3,6-trinitro-anilide) 
• 7403-13-6 acetic acid-(4-hydroxy-2.6-dinitro-anilide) 

Relevant articles and documents

Ethyl acetate as a pro-reducing agent in an one-pot reductive deamination of nitroanilines

The reductive deamination of various nitro-substituted anilines by the new method (20% H2SO4/NaNO2/ethyl acetate, Method 1) was studied and compared that with a similar procedure previously developed by Pare et al. (i.e., concentrated H2SO4/NaNO2/ethanol, Method 2) for the dediazonization of 4-methyl-2,6-dinitroaniline. The deaminated products derived from the mononitro-substituted anilines were obtained in good-to-high yield by Method 1 depending upon the position of the nitro group to the amino function. The higher yield of the de-aminated products was observed from the substituted meta-nitroanilines. Method 1 was more suitable for the deamination of 3-nitroanilines. Method 2 was more favorable for the de-amination of denitro-substituted anilines than that for the mononitroanilines. Ethyl acetate was more suitable for the reductive deamination of mononitroanilines, while ethanol was more appropriate for dinitroanilines.