329925-51-1Relevant articles and documents
Preparation of methyl 2,3-anhydro- and 2,3-o-sulfinylfuranosides from unprotected furanosides using the Mitsunobu reaction
Schulze,Voss,Adiwidjaja
, p. 229 - 234 (2001)
A new two step procedure for the synthesis of methyl 2,3-anhydro-α-D-lyxofuranoside and methyl 2,3-anhydro-β-D-ribofuranoside from D-xylose involving the intramolecular Mitsunobu reaction is presented. Likewise, methyl 2,3-anhydro-α-L-lyxofuranoside is obtained from L-arabinose. Cyclic sulfites with D-ribo configuration, synthetic equivalents of the corresponding anhydrosugars, are prepared in three steps from D-ribose.