36739-73-8Relevant articles and documents
QUATERNIZATION OF TETRAZOLES UNDER HIGH PRESSURE AND ESTABLISHMENT OF THE STRUCTURES OF QUATERNARY TETRAZOLIUM SALTS BY 13C NMR SPECTROSCOPY
Semenov, V. V.,Bogdanov, V. S.,El'yanov, B. S.,Mel'nikova, L. G.,Shevelev, S. A.,et al.
, p. 859 - 864 (1982)
The quaternization of 1- and 2-acetonyl-5-R-tetrazoles, as well as dimethyltetrazole, was accomplished under high pressure conditions (5000-14,000 kgf/cm2) by means of bromoacetone and methyl iodide and at atmospheric pressure and room temperature under the influence of methyl fluorosulfate.The structure of the salts were ascertained by 13C NMR spectroscopy, and the principles of the change in the chemical shifts and the spin-spin coupling constants during quaternization and protonation of the tetrazoles were studied.
Energetic salts of azotetrazolate, iminobis(5-tetrazolate) and 5, 5′-bis(tetrazolate)
Ye, Chengfeng,Xiao, Ji-Chang,Twamley, Brendan,Shreeve, Jean'ne M.
, p. 2750 - 2752 (2007/10/03)
Energetic ionic salts of azotetrazolate (AT), iminobis(5-tetrazolate) (IBT) and 5, 5′-bis(tetrazole) (BT) were synthesized; 1-methyl-4- aminotriazolium azotetrazolate has a layered structure and exhibits a heat of formation of 44360 kJ kg-1. The Royal Society of Chemistry 2005.