3742-63-0Relevant articles and documents
Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol
Khusainova, Narkis G.,Mostovaya, Olga A.,Azancheev, Nail M.,Litvinov, Igor A.,Krivolapov, Dmitry B.,Cherkasov, Rafael A.
, p. 212 - 214 (2004)
The reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with (rac)-butane-2,3-diol at temperatures below 0 °C leads to the formation of a hydrospirophosphorane containing both a diazaphospholene and a dioxaphospholane ring system and a β-hydroxy-alkoxy-1,2,3-diazaphospholene. On heating, these products form a hydrospirotetraoxaphosphorane, its tautomeric monocyclic β-hydroxyalkylphosphite and N-acetyl-N'-isopropylidene-hydrazine.
Catalytic hydrophosphorylation of alkyl- and acylhydrazones
Matveeva,Podrugina,Kolesnikova,Prisyazhnoi,Karateev,Zefirov
experimental part, p. 418 - 424 (2011/02/17)
N-Boc- and N-acylhydrazino phosphonates were obtained for the first time by hydrophos- phorylation of the appropriate hydrazones of aliphatic and aromatic aldehydes and heterocyclic and aliphatic ketones in the presence of [tetra(tert-butyl)phthalocyanine
1-Acyl-2-alkylhydrazines by the Reduction of Acylhydrazones
Pei-Lin-Wu,Peng, Shao-Yu,Magrath, Joe
, p. 435 - 438 (2007/10/02)
1-Acyl-2-alkylhydrazines were easily prepared by the reduction of acylhydrazones with triethylsilane in the presence of trifluoroacetic acid.