40920-09-0Relevant articles and documents
Oxidation of cis-3,5-di-tert-alkyl-3,5-diphenyl-1,2,4-trithiolanes: Isolation and some properties of the 1-oxides and the 1,2-dioxides
Oshida, Hideaki,Ishii, Akihiko,Nakayama, Juzo
, p. 5033 - 5037 (2002)
Oxidation of cis-3,5-di-tert-alkyl-3,5-diphenyl-1,2,4-trithiolane with an excess amount of dimethyldioxirane gave the 1,2-dioxide, a vic-disulfoxide, and it was verified that the 1,2-dioxide was formed specifically from one of two stereoisomeric monoxides
Deoxygenation of dithiirane 1-oxides with Lawesson's reagent leading to the corresponding dithiiranes
Ishii, Akihiko,Yamashita, Remi,Saito, Masashi,Nakayama, Juzo
, p. 1555 - 1558 (2007/10/03)
3,3-Disubstituted dithiirane 1-oxides were efficiently reduced with Lawesson's reagent (LR) to give the corresponding dithiiranes. X-ray diffraction analysis of 3,3-di(1-adamantyl)dithiirane is reported. Reaction of 34S-labeled 3,3-di(1-adamant
A new simple synthesis of cis- and trans-3,5-di-tert-butyl-3,5-diaryl-1,2,4-trithiolanes from ketones and tetraphosphorus decasulfide
Okuma,Shibata,Shioji,Yokomori
, p. 1535 - 1536 (2007/10/03)
The reaction of pivalophenones with tetraphosphorus decasulfide afforded cis- and trans-3,5-di-tert-butyl-3,5-diaryl-1,2,4-trithiolanes, which equilibrated to give other isomers in refluxing toluene via thiopivalophenones and thiopivalophe-none S-sulfides.