41866-94-8Relevant articles and documents
Synthesis and resolution of 2-hydroxyhexahelicene
Ben Braiek, Mourad,Aloui, Faouzi,Ben Hassine, Béchir
, p. 424 - 426 (2013)
2-Hydroxyhexahelicene has been prepared in good yield and purity via a three-step sequence involving palladium-catalysed Heck coupling and classical oxidative photocyclisation reactions. The two enantiomers of this hexacyclic helicenol have been separated using (S)-(-)-camphanoyl chloride as the chiral resolving agent.