42164-42-1Relevant articles and documents
Reductive debenzylation of hexabenzylhexaazaisowurtzitane
Bellamy, Anthony J.
, p. 4711 - 4722 (2007/10/02)
The reductive debenzylation of hexabenzylhexaazaisowurtzitane (2) under a wide variety of hydrogenation conditions has been investigated. Hydrogenation of 2 in acetic anhydride gives the tetraacetyl dibenzyl derivative 3 as the final product. Further acet
Synthesis of 1,3-Disubstituted Diazolidines
Lambert, Joseph B.,Huseland, Dave E.,Wang, Gen-tai
, p. 657 - 658 (2007/10/02)
Symmetrical and unsymmetrical 1,3-diaminoethanes 1 are obtained by the reduction of N,N'-disubstituted oxamides 4 with lithium aluminum hydride.The oxamides 4 are readily produced by treatment of diethyl oxalate with primary amines.The 1,3-diaminoethanes 1 lead to 1,3-diazolidines 2 on treatment with formaldehyde.