58258-66-5Relevant articles and documents
Direct cyanation of picolinamides using K4[Fe(CN)6] as the cyanide source
Guan, Dinghui,Han, Lu,Wang, Lulu,Song, He,Chu, Wenyi,Sun, Zhizhong
supporting information, p. 743 - 745 (2015/06/22)
The efficient, simple, and environment-friendly route of direct cyanation of picolinamides has been developed with nontoxic K4[Fe(CN)6] as the cyanide source through Pdcatalyzed C-H bond activation. A series of N-(naphthalene-1- yl)picolinamide derivatives were successfully transformed to the corresponding cyanation products. The cyanation mechanism has also been speculated.
Nitrogen dioxide - Sodium iodide as an efficient reagent for the one- pot conversion of aryl amines to aryl iodides under nonaqueous conditions
Suzuki, Hitomi,Nonoyama, Nobuaki
, p. 4533 - 4536 (2007/10/03)
Successive treatment of aromatic amines with liquid nitrogen dioxide and powdered sodium iodide in acetonitrile at -20 °C, followed by usual work- up, gave the corresponding aryl iodides in good yield. This method worked especially well for less basic amines bearing electron-withdrawing substituents.
SYNTHESIS OF ACETYLENIC COMPOUNDS AND BIS-α-DIKETONES ON THE BASIS OFR ACENAPHTHENE AND NAPHTHALENE DIIODIDES
Novikov, A. N.,Chaikovskii, V. K.
, p. 150 - 152 (2007/10/02)
The direct iodination of acenaphthene by the I2-HIO4 system and of naphthalene in the presence of a nitrating mixture was investigated.The direct synthesis of 2,4-diiodoacenaphthene was realized.The diiodination of naphhtalene by the iodine-nitrating mixt