634-20-8Relevant articles and documents
REINVESTIGATION OF THE SYNTHETIC REACTION OF DIMETHYLAMINO-1,3-INDANDIONE.
Ito,Abe,Sasaki,Misono
, p. 2175 - 2176 (1983)
One step preparation of dimethylamino-1,3-indandione (1) from salicyladehyde with glycine betaine was reinvestigated. Reaction conditions to give the best yield of 1, characterization of a minor product (2-acetoxybenzylidene diacetate), and reaction pathw
SiO2@FeSO4 nano composite as nanocatalyst for the green synthesis 1,1-diacetates from aldehydes under solvent-free conditions
KarimKoshteh, Mostafa,Bagheri, Marziyeh,Zeynizadeh, Behzad
, p. 2780 - 2783 (2016/07/12)
Aldehydes compounds selective converted to 1,1-diacetates as protective reagent with SiO2@FeSO4 nano composite as effective nano catalyst at room temperature under solvent-free condition and acetic anhydride (Ac2O) as acet
Poly(4-vinylpyridinium) perchlorate as an efficient solid acid catalyst for the chemoselective preparation of 1,1-diacetates from aldehydes under solvent-free conditions
Khaligh, Nader Ghaffari
, p. 329 - 334 (2014/04/03)
Poly(4-vinylpyridinium) perchlorate has been used as a supported, recyclable, environmentally-benign catalyst for the formation of acylals from aliphatic and aromatic aldehydes in good to excellent yields under solvent-free conditions. Notably, the reaction conditions were tolerant of ketones. This methodology offers several distinct advantages, including its operational simplicity and high product yield, as well as being green in terms of avoiding the use of toxic catalysts and solvents. Furthermore, the catalyst can be recovered and reused several times without any loss in its activity.