64651-83-8Relevant articles and documents
One-pot synthesis of carbamates and thiocarbamates from Boc-protected amines
Kim, Hee-Kwon,Lee, Anna
, p. 4890 - 4892 (2016/10/21)
A highly efficient one-pot procedure for the synthesis of carbamates and thiocarbamates has been described. In the presence of 2-chloropyridine and trifluoromethanesulfonyl anhydride, the isocyanate intermediates were generated in situ for further reactions with alcohols and thiols to afford the desired carbamates and thiocarbamates in high yields.
Synthesis of thiocarbamates from thiols and isocyanates under catalyst- and solvent-free conditions
Movassagh, Barahman,Soleiman-Beigi, Mohammad
, p. 137 - 140 (2008/09/20)
A simple and efficient procedure was developed for the synthesis of S-alkyl (aryl) thiocarbamates under solvent-free conditions without the use of a catalyst. The significant features of this protocol are (a) operational simplicity, (b) mild reaction cond
One-pot direct synthesis of thiocarbamates from aniline, carbon monoxide, and thiols catalyzed by selenium
Zhang, Xiaopeng,Lu, Shiwei
, p. 3291 - 3299 (2008/02/12)
Catalyzed by selenium, oxidative carbonylation of aniline and thiols with carbon monoxide and oxygen affords the corresponding thiocarbamates mostly in moderate to good yields under solvent-free conditions at ambient temperature. Copyright Taylor & Franci
