65540-54-7Relevant articles and documents
SYNTHESIS OF ETHYL 3,3-DIALKYL-3'-ALKYLSPIRO-2-CARBOXYLATES
Galin, F. Z.,Ignatyuk, V. K.,Lakeev, S. N.,Rakhimov, R. G.,Sultanova, V. S.,Tolstikov, G. A.
, p. 92 - 98 (2007/10/02)
The alkylation of indene with ultrasonic activation gave quantitative yields of 3-alkylindenes.When heated with ketones in the presence of bases, the latter gave benzofulvenes capable of entering into reaction with ethyl(dimethylsulfuranylidene)acetate with the formation of spirocyclopropane structures.A series of benzofulvenes and the corresponding ethyl 3,3-dialkyl-3'-alkylspiro-2-carboxylates were obtained.