713519-45-0Relevant articles and documents
Novel thiazole azo dye and preparation method thereof
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Paragraph 0031-0054, (2021/09/04)
The invention relates to a heterocyclic azo dye, in particular to a novel thiazole azo dye and a preparation method thereof, wherein the structural formula of the thiazole azo dye is shown as a formula (1), and the thiazole azo dye has a fluorescence quenching effect. According to the invention, strong phosphoric acid with a mass fraction of 80-85 wt% is used for dissolving a compound shown as a formula (2), strong phosphoric acid with a mass fraction of 80-85 wt% and nitrite are used for carrying out diazotization reaction on the compound shown as the formula (2), wherein the strong phosphoric acid with the mass fraction of 80-85 wt% is relatively weak in acidity, has low corrosion to equipment, improves the stability of a diazonium salt due to the influence of an acetic acid structure, and facilitates a coupling reaction of the diazonium salt and a compound shown in a formula (3), so that the yield of the thiazole azo dye shown in a formula (1) is improved.