745070-67-1

Basic information

• Product Name: 1,3,5-tris[2-methylpropionylamino]benzene
• Synonyms: 1,3,5-tris[2-methylpropionylamino]benzene
• CAS NO: 745070-67-1
• Molecular Weight: 333.431
• Mol File: 745070-67-1.mol
• Article Data: 1

Chemical Properties

• CAS DataBase Reference: 1,3,5-tris[2-methylpropionylamino]benzene(CAS DataBase Reference)
• NIST Chemistry Reference: 1,3,5-tris[2-methylpropionylamino]benzene(745070-67-1)
• EPA Substance Registry System: 1,3,5-tris[2-methylpropionylamino]benzene(745070-67-1)

Safety Data

• Hazardous Substances Data: 745070-67-1(Hazardous Substances Data)

Upstream product

• 108-72-5 1,3,5-triaminobenzene 
• 97-72-3 2-Methylpropionic anhydride 

Relevant articles and documents

Synthetic method for 1,3,5-triaminobenzene

The invention provides a synthetic method for 1,3,5-triaminobenzene. The method comprises the following steps: with phloroglucinol as shown in a structural formula IV which is described in the specification as a reaction raw material, subjecting the phloroglucinol and hydroxylamine hydrochloride to an oxime-forming reaction under an alkaline condition, and carrying out filtering and drying treatment so as to obtain 1,3,5-cyclohexanetrione oxime as shown in a structural formula III which is described in the specification; and subjecting the 1,3,5-cyclohexanetrione oxime to a hydrogenation reaction, and carrying out purification treatment so as to obtain 1,3,5-triaminobenzene as shown in a structural formula II which is described in the specification. According to the invention, a starting raw material used in the method is the phloroglucinol which is cheap and easily-available; an intermediate namely the 1,3,5-cyclohexanetrione oxime is non-explosive and facilitates separation and purification; and compared with a conventional method, the method provided by the invention has low cost and safe process. The method for preparation of the 1,3,5-triaminobenzene provided by the inventionadopts a hydrazine hydrate solution as a reducing reagent, does not need using strong acid and strong alkali, or catalytic hydrogenation under a normal pressure, and has the advantages of simple process, safety, low cost and environment friendliness.