833-64-7Relevant articles and documents
Practical acetalization and transacetalization of carbonyl compounds catalyzed by recyclable PVP-I
Cao, Fu-Rong,Lu, Guangying,Ren, Jiangmeng,Wang, Di,Zeng, Bu-Bing
, (2021/06/21)
A novel PVP-I catalyzed acetalizations/transacetalizations of carbonyl compounds has been developed processing with a mild and easy handling fashion. Different types of Acyclic and cyclic acetals were prepared from carbonyl compounds or their acetals successfully. Further applications of newly developed catalytic combination were testified. This protocol featured with simplicity of operation, mild reaction condition, short reaction time, recyclable of catalyst and broad substrates scope with excellent yields.
Synthesis and characterization of a tetracationic acidic organic salt and its application in the synthesis of bis(indolyl)methanes and protection of carbonyl compounds
Halimehjani, Azim Ziyaei,Hooshmand, Seyyed Emad,Shamiri, Elham Vali
, p. 21772 - 21777 (2015/03/18)
A new tetracationic acidic organic salt (TCAOS) based on DABCO was prepared, characterized and applied as an eco-friendly, powerful and reusable catalyst for the synthesis of bis(indolyl)methanes from indoles and carbonyl compounds in water with high turnover frequency (TOF). Also, this catalyst was successfully applied for acetalization of carbonyl compounds with diols under solvent-free conditions.
Microwave-assisted synthesis and bioactivity of some 2- dichloromethyl-1,3-dioxacycloalkanes
Ye, Fei,Sun, Chang-Ying,Zhao, Li-Xia,Li, Ying,Fu, Ying
, p. 159 - 164 (2019/01/21)
A series of 2-dichloromelhyl-1,3-dioxacycloalkanes (3) was synthesized by microwave-assisted cyclization and insertion reaction. All the compounds were characterized by IR, 1H NMR, 13C NMR, MS and elemental analysis. The single crystal of compound (3b) was determined by X-ray crystallographic analysis. The preliminary bioassay results demonstrated that these compounds could alleviate acetochlor injury to maize.