86166-00-9Relevant articles and documents
Synthesis of the Radical Scavenger 1,1,3,3-Tetramethylisoindolin-2-yloxyl
Griffiths, Peter G.,Moad, Graeme,Rizzardo, Ezio,Solomon, David H.
, p. 397 - 401 (2007/10/02)
A versatile free-radical trapping agent, 1,1,3,3-tetramethylisoindolin-2-yloxyl, has been prepared from N-benzylphthalimide by reaction with 'methylmagnesium iodide' in refluxing toluene followed by hydrogenolysis and oxidation.The Grignard reaction gives 2-benzyl-1,1,3,3-tetramethylisoindoline along with a small proportion of an unexpected by-product, 2-benzyl-1-ethyl-1,3,3-trimethylisoindoline.
