940447-63-2

Basic information

• Product Name: N-(4-methoxyphenyl)-3,5-dinitro-N-(phenylsulfonyl)benzamide
• CAS NO: 940447-63-2
• Molecular Weight: 457.42
• Mol File: 940447-63-2.mol
• Article Data: 1

Chemical Properties

• CAS DataBase Reference: N-(4-methoxyphenyl)-3,5-dinitro-N-(phenylsulfonyl)benzamide(CAS DataBase Reference)
• NIST Chemistry Reference: N-(4-methoxyphenyl)-3,5-dinitro-N-(phenylsulfonyl)benzamide(940447-63-2)
• EPA Substance Registry System: N-(4-methoxyphenyl)-3,5-dinitro-N-(phenylsulfonyl)benzamide(940447-63-2)

Safety Data

• Hazardous Substances Data: 940447-63-2(Hazardous Substances Data)

Upstream product

• 7471-26-3 N-(4-methoxyphenyl)benzenesulphonamide 
• 99-33-2 3,5-dinitrobenoyl chloride 

Relevant articles and documents

An efficient method for the synthesis of N-acylsulfonamides: One-pot sulfonylation and acylation of primary arylamines under solvent-free conditions

The preparation of N-acylsulfonamides is described using primary amines, arylsulfonyl chlorides and acyl chlorides. Reaction of primary aryl amines with arylsulfonyl chlorides in the presence of NaHCO3 produced N-arylsulfonamides, which reacted in situ with benzoyl chloride furnishing the corresponding N-benzoyl-N-arylsulfonamides in 72-96% yields. Accordingly, 4-nitrobenzoyl chloride and 3,5-dinitrobenzoyl chloride were used as acylating agents. All the reactions were carried out under solvent-free conditions at room temperature and the products were isolated after simple work-up in high yields and purity.