96501-85-8Relevant articles and documents
First total synthesis of medicinally important 3,4,7-trimethoxy-9,10-dihydrophenanthrene-1,5-diol
Gangireddy Venkata, Sivarami Reddy,Narkhede, Umesh C.,Jadhav, Vinod D.,Gangu Naidu, Ch.
, p. 1670 - 1673 (2018/03/29)
The first total synthesis was successfully achieved for biologically active 9,10-dihydrophenanthrene-1,5-diol. The key features of our synthetic approach are Perkin condensation, followed by bromination, palladium mediated intramolecular C-C bond coupling, and selective isopropyl ether cleavage. Synthesized compounds were purified and characterized by IR, 1HNMR, 13CNMR and HRMS/LC-MS.
Synthetic studies on flavone derivatives. XIV. Synthesis of 2',4'-5'-trioxygenated flavones
Iinuma,Iwashima,Matsuura
, p. 4935 - 4941 (2007/10/02)
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