98170-72-0Relevant articles and documents
Ultrasound in Phosphine Preparation. Simple Preparations of Some Bis(alkylphenylphosphino)alkanes
Chou, Ta-shue,Tsao, Chung-Huang,Hung, Su Chun
, p. 4329 - 4332 (1985)
Diphosphines of the class RPhP(CH2)nPPhR (n=2-6) have been prepared from reactions of the corresponding Ph2P(CH2)nPPh2 with alkali metall followed by alkylation.Ultrasound irradiation should be applied in the reductive cleavage stage so as to assure the purity of the final products.