988-19-2Relevant articles and documents
Synthesis of α,β-unsaturated ketone from α-iodo ketone using photoirradiation
Ji, Shun-Jun,Takahashi, Eiji,Takahashi, T. Tomoyoshi,Horiuchi, C. Akira
, p. 9263 - 9266 (2007/10/03)
Irradiation of α-iodo ketone in hexane under a nitrogen atmosphere with a high-pressure mercury lamp (λ>300nm) at room temperature afforded the corresponding α,β-unsaturated ketones in good yield. This reaction affords a new, clean and convenient synthetic method for the α,β-unsaturated ketone.